Ftir analysis and elemental mapping services with Microvisionlabs.com? As indicated in the FTIR spectral comparison below, the suspect material showed a near perfect match for acetylsalicylic acid. Additionally, there was a small amount of dibasic phosphate present. It was determined that the material was likely acetylsalicylic acid with a phosphate binder – an aspirin. Therefore, from this analysis the suspect material in the bottle was likely a household aspirin tablet, broken apart and separated by the water. In order to confirm the identification, a few aspirin tablets from several common manufacturers were obtained, roughly ground, and soaked to allow for comparison. The optical morphology of the crystals, size range of the particles, association with the phosphate and FTIR spectrum all were consistent with the original suspect material. A report detailing the methods and findings in full narrative form was rendered to the client.
SEM is a powerful surface microscopy method which allows for high resolution images to be obtained on a wide range of samples. A focused beam of electrons sweeps across a sample surface and an image is created from the scattered electrons. The electron beam allows for the accurate imaging of features below the resolution limit of visible light. The acquired pictures retain good depth of field, resulting in excellent three-dimensional images. Variations in beam parameters can be made in order to highlight variations in density in the target sample, show extremely fine surface features, and illustrate texture in sample surface coatings. MicroVision Labs has multiple fully-operational SEMs, Bruker X-Flash EDS detectors and mapping technology, backscatter electron (BSE) imaging, and large chamber capabilities. These provide a full suite of microscopy services for all of your analytical needs.
What is your standard turnaround time (TAT) and can it be expedited? Our standard TAT is 5 to 10 business days. We can provide faster TATs on request with the following surcharges: – Same day to 24 hour rush is 100% surcharge – 2 day rush is 75% surcharge – 3 day rush is 50% surcharge – 4 day rush is 25% surcharge Rush requests must have prior approval otherwise we cannot guarantee turnaround times. Find extra info at info on elemental labs.
The scan from left to right shows a high tin concentration (green line) while areas of higher lead concentrations (blue line) were not intersected by the line scan. At the interface between the tin/lead solder and copper (red line), there is a mixture of the solder and copper which is the intermetallic layer. The EDS Map provides a nice visual mixture of colors which shows the intermetallic layer while the line scan clearly shows the intermetallic with the elemental graph.
MicroVision Laboratories, Inc. has been providing extensive expertise in micro-analytical techniques (FE-SEM, SEM, EDS, XRF, FTIR testing, PLM, X-Ray Imaging, DIC) and sample preparation since 2003. Our cutting edge, high-performance equipment combined with our solutions-focused customer service provide critical solutions for clients hailing from a broad range of industries ranging from medical to semiconductor, and from environmental to textile.
Examining the sample with a polarized light microscope (PLM), it was darker and coarser than expected for a mold sample. The dust appeared to be a closed cell, synthetic blown foam material, and all from the same source. The black color was likely due to pigment particles added to color the foam. Fourier Transform Infra-Red spectroscopy was performed on the foam particles. The spectrum showed a mixture of spectral features, associated with vinyl acetates, polyurethane, and cellulose or other sugar-like polymers. Based on these features, a common urethane acetate foam was determined as the likely source material. Read more details on https://microvisionlabs.com/.